Mechanochemical synthesis of N-doped porous carbon at room temperature

Mirian Elizabeth Casco; Sebastian Kirchhoff; Desirée Leistenschneider; Marcus Rauche; Eike Brunner; Lars Borchardt

doi:10.1039/c9nr01019j

Mechanochemical synthesis of N-doped porous carbon at room temperature

Mirian Elizabeth Casco
, Sebastian Kirchhoff
, Desirée Leistenschneider
, Marcus Rauche
, Eike Brunner
, Lars Borchardt

TU Dresden

Research output: Contribution to journal › Article › peer-review

51 Scopus citations

Abstract

We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m² g^-1.

Original language	English
Pages (from-to)	4712-4718
Number of pages	7
Journal	Nanoscale
Volume	11
Issue number	11
DOIs	https://doi.org/10.1039/c9nr01019j
State	Published - 21 Mar 2019
Externally published	Yes

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10.1039/c9nr01019j

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abstract = "We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt\% of nitrogen and exhibiting a surface area of 1080 m2 g-1.",

author = "Casco, \{Mirian Elizabeth\} and Sebastian Kirchhoff and Desir{\'e}e Leistenschneider and Marcus Rauche and Eike Brunner and Lars Borchardt",

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AU - Casco, Mirian Elizabeth

AU - Kirchhoff, Sebastian

AU - Leistenschneider, Desirée

AU - Rauche, Marcus

AU - Brunner, Eike

AU - Borchardt, Lars

PY - 2019/3/21

Y1 - 2019/3/21

N2 - We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m2 g-1.

AB - We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m2 g-1.

UR - https://www.scopus.com/pages/publications/85062857956

U2 - 10.1039/c9nr01019j

DO - 10.1039/c9nr01019j

M3 - Artículo

C2 - 30838363

AN - SCOPUS:85062857956

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JO - Nanoscale

JF - Nanoscale

IS - 11

ER -

Mechanochemical synthesis of N-doped porous carbon at room temperature

Abstract

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